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LC Multiresidue Pesticide Standard #4 on Raptor ARC-18 by LC-MS/MS
| Peaks | tR (min) | Precursor Ion | Product Ion 1 | Product Ion 2 | |
|---|---|---|---|---|---|
| 1. | Cyromazine | 1.07 | 167.0 | 85.0 | 108.1 |
| 2. | Pymetrozine | 1.35 | 218.0 | 105.0 | 79.0 |
| 3. | Dinotefuran | 1.63 | 203.0 | 129.0 | 157.0 |
| 4. | Nitenpyram | 1.68 | 271.1 | 125.9 | 224.9 |
| 5. | Flonicamid | 1.89 | 230.0 | 203.1 | 174.1 |
| 6. | Imidacloprid | 2.19 | 256.1 | 175.1 | 209.1 |
| 7. | Acetamiprid | 2.40 | 223.0 | 126.0 | 56.1 |
| 8. | Cymoxanil | 2.47 | 199.0 | 128.0 | 111.0 |
| 9. | Oxadixyl | 2.77 | 279.0 | 219.0 | 132.0 |
| 10. | Carbetamide | 2.79 | 237.0 | 118.0 | 192.0 |
| 11. | Secbumeton | 2.93 | 226.2 | 100.2 | 170.2 |
| 12. | Prometon | 2.93 | 226.0 | 86.3 | 184.3 |
| 13. | Terbumeton | 2.97 | 226.1 | 114.1 | 170.1 |
| 14. | Imazalil | 2.97 | 297.0 | 159.0 | 69.0 |
| 15. | Pyracarbolid | 3.04 | 218.1 | 125.1 | 97.1 |
| 16. | Ametryn | 3.22 | 228.1 | 68.1 | 186.1 |
| 17. | Pyrimethanil | 3.51 | 200.0 | 107.0 | 82.0 |
| 18. | Spiroxamine isomer 1 | 3.56 | 298.0 | 144.0 | 100.0 |
| 19. | Metalaxyl | 3.56 | 280.1 | 220.1 | 192.1 |
| 20. | Spiroxamine isomer 2 | 3.62 | 298.0 | 144.0 | 100.0 |
| 21. | Chlorantraniliprole | 3.66 | 483.9 | 286.0 | 453.0 |
| 22. | Azoxystrobin | 3.92 | 404.1 | 372.0 | 329.0 |
| 23. | Furalaxyl | 3.96 | 302.1 | 270.1 | 242.2 |
| 24. | Fludioxonil | 3.97 | 249.1 | 229.1 | 158.1 |
| 25. | Halofenozide | 3.98 | 331.1 | 104.9 | 275.0 |
| 26. | Boscalid | 4.06 | 342.9 | 307.0 | 139.9 |
| 27. | Mandipropamid | 4.08 | 412.3 | 328.2 | 356.2 |
| 28. | Flutolanil | 4.10 | 324.1 | 262.1 | 65.0 |
| 29. | Mepronil | 4.20 | 270.1 | 91.0 | 119.0 |
| 30. | Myclobutanil | 4.25 | 289.1 | 125.1 | 70.2 |
| 31. | Methoxyfenozide | 4.29 | 369.1 | 149.1 | 313.2 |
| 32. | Triadimefon | 4.33 | 294.1 | 197.2 | 69.3 |
| 33. | Cyprodinil | 4.34 | 226.0 | 93.0 | 108.0 |
| 34. | Mepanipyrim | 4.40 | 224.1 | 106.0 | 77.0 |
| 35. | Fenhexamid | 4.46 | 302.1 | 97.2 | 55.3 |
| 36. | Fluoxastrobin | 4.46 | 459.0 | 427.0 | 188.0 |
| 37. | Butafenacil | 4.48 | 492.0 | 180.0 | 331.0 |
| 38. | Picoxystrobin | 4.78 | 368.0 | 145.1 | 205.1 |
| 39. | Rotenone | 4.83 | 395.0 | 213.1 | 192.1 |
| 40. | Tebufenozide | 4.86 | 353.1 | 133.0 | 297.1 |
| 41. | Dimoxystrobin | 4.87 | 327.1 | 116.1 | 205.2 |
| 42. | Carfentrazone ethyl | 4.89 | 412.0 | 346.0 | 266.0 |
| 43. | Kresoxim-methyl | 4.90 | 314.1 | 206.0 | 116.0 |
| 44. | Zoxamide | 5.06 | 336.0 | 187.1 | 159.0 |
| 45. | Famoxadone | 5.09 | 392.2 | 331.1 | 238.0 |
| 46. | Prochloraz | 5.14 | 376.0 | 308.0 | 70.1 |
| 47. | Benalaxyl | 5.15 | 326.1 | 148.0 | 91.0 |
| 48. | Clofentezine | 5.21 | 303.0 | 138.0 | 102.0 |
| 49. | Benzoximate | 5.28 | 364.0 | 199.1 | 105.0 |
| 50. | Trifloxystrobin | 5.50 | 409.0 | 186.0 | 145.0 |
| 51. | Fluazinam | 5.77 | 464.8 | 373.0 | 338.1 |
| 52. | Metaflumizone | 5.79 | 507.0 | 287.2 | 267.1 |
| 53. | Tebufenpyrad | 5.85 | 334.0 | 117.0 | 145.0 |
| 54. | Pyriproxifen | 5.91 | 322.1 | 96.0 | 227.1 |
| 55. | Piperonyl butoxide | 5.93 | 356.3 | 176.9 | 119.0 |
| 56. | Quinoxyfen | 6.03 | 308.0 | 197.0 | 161.9 |
| 57. | Amitraz | 6.14 | 294.0 | 163.0 | 122.0 |
| 58. | Fenpyroximate | 6.36 | 422.2 | 138.1 | 366.1 |
| 59. | Abamectin B1b | 6.47 | 876.6 | 553.4 | 291.0 |
| 60. | Eprinomectin | 6.53 | 914.6 | 186.0 | 154.0 |
| 61. | Abamectin B1a | 6.61 | 890.5 | 305.2 | 567.3 |
| 62. | Fenazaquin | 6.68 | 307.2 | 161.0 | 57.2 |
| 63. | Doramectin | 6.81 | 916.6 | 331.2 | 593.4 |
| 64. | Moxidectin | 6.81 | 640.5 | 498.3 | 528.4 |
| 65. | Ivermectin | 7.00 | 892.6 | 569.4 | 551.4 |
Isomers are numbered sequentially based on elution order.
LC_FF0546
| Column | Raptor ARC-18 (cat.# 9314A12) | ||||||||||||||||||||||||||||||||
| Dimensions: | 100 mm x 2.1 mm ID | ||||||||||||||||||||||||||||||||
| Particle Size: | 2.7 µm | ||||||||||||||||||||||||||||||||
| Temp.: | 50 °C | ||||||||||||||||||||||||||||||||
| Sample | LC multiresidue pesticide standard #4 (cat.# 31975) | ||||||||||||||||||||||||||||||||
| Diluent: | Water | ||||||||||||||||||||||||||||||||
| Conc.: | 20 ng/mL | ||||||||||||||||||||||||||||||||
| Inj. Vol.: | 5 µL | ||||||||||||||||||||||||||||||||
| Mobile Phase | |||||||||||||||||||||||||||||||||
| A: | Water + 2 mM ammonium formate + 0.2% formic acid | ||||||||||||||||||||||||||||||||
| B: | Methanol + 2 mM ammonium formate + 0.2% formic acid | ||||||||||||||||||||||||||||||||
| |||||||||||||||||||||||||||||||||
| Detector | Waters Xevo TQ-S | ||||||||||||||||||||||||||||||||
| Ion Source: | Waters Zspray™ ESI | ||||||||||||||||||||||||||||||||
| Ion Mode: | ESI+ | ||||||||||||||||||||||||||||||||
| Mode: | MRM | ||||||||||||||||||||||||||||||||
| Instrument | Waters | ||||||||||||||||||||||||||||||||
| Notes | Autosampler Temperature = 5 °C |
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