Innovative Chromatography Products
www.restek.fr
www.restek.fr
Analysis of Mycotoxins on Raptor FluoroPhenyl by LC-MS/MS
| Peaks | tR (min) | Conc. (ng/mL) | Precursor Ion | Product Ion | Product Ion | |
|---|---|---|---|---|---|---|
| 1. | Nivalenol | 1.04 | 100 | 313.22 | 175.09 | 91.08 |
| 2. | Patulin | 1.42 | 50 | 155.00 | 98.94 | 80.98 |
| 3. | Deoxynivalenol | 1.53 | 50 | 297.20 | 249.04 | 231.03 |
| 4. | Fusarenon X | 2.13 | 100 | 355.20 | 247.10 | 175.08 |
| 5. | 15-Acetyldeoxynivalenol | 3.07 | 100 | 339.23 | 321.15 | 137.07 |
| 6. | 3-Acetyldeoxynivalenol | 3.22 | 100 | 339.16 | 231.10 | 213.08 |
| 7. | Aflatoxin M1 | 4.11 | 25 | 329.22 | 273.09 | 229.12 |
| 8. | Diacetoxyscirpenol | 4.41 | 100 | 367.24 | 307.14 | 105.07 |
| 9. | Aflatoxin G2 | 4.67 | 25 | 331.16 | 313.00 | 189.01 |
| 10. | Aflatoxin G1 | 4.87 | 25 | 329.13 | 243.00 | 199.74 |
| 11. | HT-2 | 4.92 | 50 | 447.20 | 345.08 | 285.11 |
| 12. | Aflatoxin B2 | 5.20 | 25 | 315.13 | 287.02 | 258.98 |
| 13. | Aflatoxin B1 | 5.32 | 25 | 313.16 | 284.85 | 241.06 |
| 14. | Citrinin | 5.38 | 10 | 251.15 | 233.09 | 205.05 |
| 15. | Fumonisin B1 | 5.56 | 25 | 722.46 | 352.25 | 334.23 |
| 16. | T-2 | 5.63 | 50 | 489.24 | 245.07 | 387.12 |
| 17. | Fumonisin B3 | 6.03 | 25 | 706.43 | 336.23 | 318.29 |
| 18. | Ochratoxin A | 6.17 | 25 | 404.07 | 238.96 | 357.98 |
| 19. | Fumonisin B2 | 6.31 | 25 | 706.43 | 336.23 | 318.29 |
| 20. | Zearalenone | 6.44 | 50 | 319.23 | 283.06 | 187.04 |
LC_FS0511
| Column | Raptor FluoroPhenyl (cat.# 9319A12) | ||||||||||||||||||||
| Dimensions: | 100 mm x 2.1 mm ID | ||||||||||||||||||||
| Particle Size: | 2.7 µm | ||||||||||||||||||||
| Pore Size: | 90 Å | ||||||||||||||||||||
| Guard Column: | Raptor FluoroPhenyl EXP guard column cartridge 5 mm, 2.1 mm ID, 2.7 µm (cat.# 9319A0252) | ||||||||||||||||||||
| Temp.: | 30 °C | ||||||||||||||||||||
| Sample | |||||||||||||||||||||
| Diluent: | Water:methanol (80:20) | ||||||||||||||||||||
| Conc.: | 10-100 ng/mL | ||||||||||||||||||||
| Inj. Vol.: | 5 µL | ||||||||||||||||||||
| Mobile Phase | |||||||||||||||||||||
| A: | 0.3% Formic acid in water | ||||||||||||||||||||
| B: | Methanol | ||||||||||||||||||||
| |||||||||||||||||||||
| Max Pressure: | 525 bar | ||||||||||||||||||||
| Detector | MS/MS | ||||||||||||||||||||
| Ion Mode: | ESI+ | ||||||||||||||||||||
| Mode: | MRM | ||||||||||||||||||||
| Instrument | UHPLC |
RECHERCHES SIMILAIRES
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